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Several Gold's reagents were synthesized from cyanuric chloride and N,N-dialkylformamides.These synthetic equivalents of N,N-dimethylformamide dimethyl acetal were used in an optimized and scalable procedure for the regioselective synthesis of a variety of enaminones from ketone starting materials, whose utility was demonstrated by the stereoselective synthesis of Rawal-type dienes.
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The dienophile used in this experiment was Maleic anhydride ( a cyclic dienophile ) and the diene used was cyclopentadiene ( a cyclic diene ). Due to the fact that more than one stereoisomer may organize. it is of import to cognize that the major merchandise will be the 1 with the passage province for the endo stereochemistry while the minor merchandise will be for the exo stereochemistry.